utopian77 Posted July 21 Report Share Posted July 21 but I ain't got no sh*t - any assistance? Quote Link to comment Share on other sites More sharing options...
Randy Posted July 21 Report Share Posted July 21 find a big hill or rent a car Quote Link to comment Share on other sites More sharing options...
gadzinm Posted July 21 Report Share Posted July 21 Tuck the chin and kick the heels!!!! Repeat over and over!!!![This message has been edited by airwave1 (edited 07-21-2000).] Quote Link to comment Share on other sites More sharing options...
muthaload Posted July 21 Report Share Posted July 21 Dude, everyone and there mother sells E, i'm sure if you look hard enough youll find somebody. Please anyone that doesnt sell E dont take offense. Quote Link to comment Share on other sites More sharing options...
apdiddy Posted July 21 Report Share Posted July 21 look for me wherever you go tonite. i'll be the huge guy with a STAFF shirt on.------------------deez nuts Quote Link to comment Share on other sites More sharing options...
back2basics Posted July 21 Report Share Posted July 21 Make your own.MDMA Synthesis: Bromosafrole methodScanned fom _Secrets of Mthamphetamine Maufacture_ A good alternative to the Ritter reaction is a two step procedurefirst reacting safrole with hydrobromic acid to give 3,4-methylenedi-oxyphenyl-2-bromopropane, and then taking this material and reactingit with either ammonia or methylamine to yield MDA or MDMArespectively. This procedure has the advantages of not being at allsensitive to batch size, nor is it likely to "run away" and produce atarry mess. It shares with the Ritter reaction the advantage of usingcheap, simple, and easily available chemicals. The sole disadvantage of this method is the need to do the finalreaction with ammonia or methylamine inside a sealed pipe. This isbecause the reaction must be done in the temperature range of 120-140 C, and the only way to reach this temperature is to seal thereactants up inside of a bomb. This is not particularly dangerous, andis quite safe if some simple precautions are taken. The first stage of the conversion, the reaction with hydrobromicacid, is quite simple, and produces almost a 100% yield of the bromi-nated product. See the Journal of Biological Chemistry, Volume 108page 619. The author is H.E. Carter. Also see Chemical Abstracts1961, column 14350. The following reaction takes place:[ Structural diagrams deleted] To do the reaction, 200 ml of glacial acetic acid is poured into achampagne bottle nestled in ice. Once the acetic acid has cooleddown, 300 grams (200 ml) of 48% hydrobromic acid is slowly addedwith swirling. Once this mixture has cooled down, 100 grarns ofsafrole is slowly added with swirling. Once the safrole is added, thecheap plastic stopper of the champagne bottle is wired back intoplace, and the mixture is slowly allowed to come to room temperaturewith occasional shaking. After about 12 hours the original two layerswill merge into a clear red solution. In 24 hours, the reaction is done.The chemist carefully removes the stopper from the bottle, wearingeye protection. Some acid mist may escape from around the stopper. The reaction mixture is now poured onto about 500 grams ofcrushed ice in a 1000 or 2000 ml beaker. Once the ice has melted, thered layer of product is separated, and the water is extracted with aboutl00 ml of petroleum ether or regular ethyl ether. The ether extract isadded to the product, and the combined product is washed first withwater, and then with a solution of sodium carbonate in water. Thepurpose of these washings is to remove HBr from the product. Onecan be sure that all the acid is removed from the product when somefresh carbonate solution does not fizz in contact with the product. Once all the acid in the product is removed, the ether must beremoved from it. This is important because if the ether were allowedto remain in it, too much pressure would be generated in the nextstage inside of the bomb. Also, it would interfere with the formationof a solution between the product and methylamine or ammonia. It isnot necessary to distill the product because with a yield of over 90%,the crude product is pure enough to feed into the next stage. Toremove the ether from the product, the crude product is poured into aflask, and a vacuum is applied to it. This causes the ether to boil off.Some gentle heating with hot water is quite helpful to this process.The yield of crude product is in the neighborhood of 200 grams. With the bromo compound in hand, it is time to move onto thenext step which gives MDA or MDMA. See Chemical Abstracts1961, column 14350. Also see Journal of the American ChemicalSociety, Volume 68, page 1805 and Journal of the Chemistry Society,part 2 1938, page 2005. The bromo compound reacts with ammoniaor methylamine to give MDA or MDMA:[ Sructural diagram deleted ] To do the reaction, 50 grams of the bromo compound is pouredinto a beaker, and 200 ml of concentrated ammonium hydroxide (28%NH3) or 40% methylamine is added. Next, isopropyl alcohol is addedwith stirring until a nice smooth solution is formed. It is not good toadd too much alcohol because a more dilute solution reacts slower.Now the mixture is poured into a pipe "bomb." This pipe should bemade of stainless steel, and have fine threads on both ends. Stainlesssteel is preferred because the HBr given off in the reaction will rustregular steel. Both ends of the pipe are securely tightened down. Thebottom may even be welded into place. Then the pipe is placed intocooking oil heated to around 130 C. This temperature is maintainedfor about 3 hours or so, then it is allowed to cool. Once the pipe ismerely warm, it is cooled down some more in ice, and the capunscrewed. The reaction mixture is poured into a distilling flask, the glass-ware rigged for simple distillation, and the isopropyl alcohol andexcess ammonia or methylamine is distilled off. When this is done,the residue inside the flask is made acid with hydrochloric acid. Ifindicating pH paper is available, a pH of about 3 should be aimed for.This converts the MDA to the hydrochloride which is water soluble.Good strong shaking of the mixture ensures that this conversion iscomplete. The first stage of the purification is to recover unreactedbromo compound. To do this, 200 to 300 ml of ether is added. Aftersome shaking, the ether layer is separated. It contains close to 20grams of bromo compound which may be used again in later batches. Now the acid solution containing the MDA is made strongly basicwith lye solution. The mixture is shaken for a few minutes to ensurethat the MDA is converted to the free base. Upon sitting for a fewminutes, the MDA floats on top of the water as a dark colored oilylayer. This layer is separated and placed into a distilling flask. Next,the water layer is extracted with some toluene to get out the remainingMDA free base. The toluene is combined with the free base layer, andthe toluene is distilled off. Then a vacuum is applied, and the mixtureis fractionally distilled. A good aspirator with cold water will bringthe MDA off at a temperature of 150 to 160 C. The free base shouldbe clear to pale yellow, and give a yield of about 20 ml. This free baseis made into the crystalline hydrochloride by dissolving it in ether andbubbling dry HCl gas through it. Quote Link to comment Share on other sites More sharing options...
trance604 Posted July 21 Report Share Posted July 21 you definetely wont get an answer from somone that reads, i have it call me at 718-555-6789 x252 between 8-12 tonite. bee a little discreet about it, or get to a club and make friends, unfortunately i hate clubs as of late but i might change that... Quote Link to comment Share on other sites More sharing options...
frankie_pep Posted July 21 Report Share Posted July 21 Originally posted by vj604:you definetely wont get an answer from somone that reads, i have it call me at 718-555-6789 x252 between 8-12 tonite. bee a little discreet about it, or get to a club and make friends, unfortunately i hate clubs as of late but i might change that...ARE YOU FUCKING SERIOUS??? ... If sO yOu gOt bIg bAllZ ... Quote Link to comment Share on other sites More sharing options...
muthaload Posted July 21 Report Share Posted July 21 ELEPHANT SIZE BALLS!!!! Quote Link to comment Share on other sites More sharing options...
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